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Spinnovation facilities consist of the following intruments:
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solution NMR
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NMR probes
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- 500MHz (+ sample changer)
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- 5mm ATM TCI-cryo-cooled
- 5mm ATM BBI
- LC-NMR / LC-SPE-NMR (30µL)
- BEST-NMR (120µL)
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- 5mm TXI HCN-XYZ gradients
- 5mm TXI HCP-XYZ gradients
- 5mm TXI HCX-Z gradient
- 5mm BBO HX
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- 5mm TXI HCN-Z gradient cryo-cooled
- 5mm TXI HCN with PFG
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solid-state NMR
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NMR probes
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- 2.5mm CP-MAS (spinning 35 kHz)
- 4mm CP-MAS triple resonance
- 10mm (15N-27Al) CP-MAS (spinning up to 5 kHz)
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- 2.5mm BB CP-MAS (spinning 30 kHz)
- 3.2mm BB CP-MAS (spinning 25 kHz)
- 6mm BB CP-MAS (spinning 12 kHz)
- 4mm CP-MAS triple
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- 2.5mm BB CP-MAS (spinning 30 kHz)
- 3.2mm BB (T3) CP-MAS (spinning 25 kHz)
- 4mm triple HXY (T3)
- 4mm HFXY (T3) CP-MAS (spinning 18 kHz)
- 6mm Low Gamma probe
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- 850 MHz, to be installed end 2009
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Mass Spectrometry
- Esi-Tof (accurate mass)
- LC-ESI-Tof (accurate mass)
- LC-SPE-ESI-Tof (accurate mass)
Systems for sample preparation / separation
- Liquid sample handler Gilson (full automation sample prep. and injection to NMR and MS)
- HPLC Agilent 1200 (UV detector VW, 2x96 well-plate sample changer)
- Solid-phase extraction system Prospek 2, 2x96 columns
- Glove-box
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